{"id":55866,"date":"2002-02-01T00:00:00","date_gmt":"2018-12-04T06:07:03","guid":{"rendered":"https:\/\/aprifel-pp.mentalworks.biz\/fr\/resume-scientifique\/determination-of-fungicide-residues-in-fruits-and-vegetables\/"},"modified":"2018-12-04T07:07:03","modified_gmt":"2018-12-04T06:07:03","slug":"determination-of-fungicide-residues-in-fruits-and-vegetables","status":"publish","type":"resume","link":"https:\/\/aprifel-pp.mentalworks.biz\/fr\/resume-scientifique\/determination-of-fungicide-residues-in-fruits-and-vegetables\/","title":{"rendered":"Determination of fungicide residues in fruits and vegetables by liquid chromatography-atmospheric pressure chemical ionization mass spectrometry"},"content":{"rendered":"<p>A liquid chromatography (LC) method for the quantitative determination of five fungicide residues (dichloran, flutriafol, o-phenylphenol, prochloraz and tolclofos methyl) in oranges, lemons, bananas, peppers, chards and onions is described. The residues were extracted by matrix solid-phase dispersion (MSPD) using C-8. Quantitative analysis was performed by isocratic LC coupled to quadrupole mass spectrometer using atmospheric pressure chemical ionization in the negative ionization mode. The limit of quantification was 0.01 mg\/kg for flutiiafol, o-phenylphenol and dichloran, and 0.1 mg\/kg for prochloraz and tolclofos methyl. The MSPD method is also suitable for LC-UV analysis but higher limits of quantification (between 1 and 5 mg\/kg) were obtained. Validation of the method was performed between 0.01 and 25 mg\/kg. Recoveries for fungicides ranged from 52.5 to 91.1% with relative standard deviations between 6.1 and 11.9%. The method was applied to the determination of residues in samples taken from agricultural cooperatives. The fungicides most often detected were o-phenylphenol and prochloraz.<\/p>\n","protected":false},"template":"","mots_cles":[],"class_list":["post-55866","resume","type-resume","status-publish","hentry"],"acf":{"adresse":"PICO Y,UNIV VALENCIA,FAC FARM LAB BROMATOL & TOXICOL;AV VICENT ANDRES ESTELLES S-N; VALENCIA 46100, SPAIN.pico@uv.es","annee":"2002","mois":"2","numero":"947:2 227-235 FEB 22 2002","page":"227-235","auteurs":[{"ID":20015,"post_author":"0","post_date":"2018-12-03 20:29:21","post_date_gmt":"2018-12-03 19:29:21","post_content":"","post_title":"Jordi Ma\u00f1es","post_excerpt":"","post_status":"publish","comment_status":"closed","ping_status":"closed","post_password":"","post_name":"jordi-manes","to_ping":"","pinged":"","post_modified":"2018-12-03 20:29:21","post_modified_gmt":"2018-12-03 19:29:21","post_content_filtered":"","post_parent":0,"guid":"https:\/\/aprifel-pp.mentalworks.biz\/fr\/auteur\/jordi-manes\/","menu_order":0,"post_type":"auteur_resume","post_mime_type":"","comment_count":"0","filter":"raw"},{"ID":40861,"post_author":"0","post_date":"2018-12-04 02:23:15","post_date_gmt":"2018-12-04 01:23:15","post_content":"","post_title":"Pico","post_excerpt":"","post_status":"publish","comment_status":"closed","ping_status":"closed","post_password":"","post_name":"pico","to_ping":"","pinged":"","post_modified":"2018-12-04 02:23:15","post_modified_gmt":"2018-12-04 01:23:15","post_content_filtered":"","post_parent":0,"guid":"https:\/\/aprifel-pp.mentalworks.biz\/fr\/auteur\/pico\/","menu_order":0,"post_type":"auteur_resume","post_mime_type":"","comment_count":"0","filter":"raw"},{"ID":14556,"post_author":"0","post_date":"2018-12-03 19:11:08","post_date_gmt":"2018-12-03 18:11:08","post_content":"","post_title":"Guillermina Font","post_excerpt":"","post_status":"publish","comment_status":"closed","ping_status":"closed","post_password":"","post_name":"guillermina-font","to_ping":"","pinged":"","post_modified":"2018-12-03 19:11:08","post_modified_gmt":"2018-12-03 18:11:08","post_content_filtered":"","post_parent":0,"guid":"https:\/\/aprifel-pp.mentalworks.biz\/fr\/auteur\/guillermina-font\/","menu_order":0,"post_type":"auteur_resume","post_mime_type":"","comment_count":"0","filter":"raw"},{"ID":55865,"post_author":"0","post_date":"2018-12-04 07:07:02","post_date_gmt":"2018-12-04 06:07:02","post_content":"","post_title":"Blasco","post_excerpt":"","post_status":"publish","comment_status":"closed","ping_status":"closed","post_password":"","post_name":"blasco","to_ping":"","pinged":"","post_modified":"2018-12-04 07:07:02","post_modified_gmt":"2018-12-04 06:07:02","post_content_filtered":"","post_parent":0,"guid":"https:\/\/aprifel-pp.mentalworks.biz\/fr\/auteur\/blasco\/","menu_order":0,"post_type":"auteur_resume","post_mime_type":"","comment_count":"0","filter":"raw"}],"sources":[{"ID":53445,"post_author":"0","post_date":"2018-12-04 06:19:18","post_date_gmt":"2018-12-04 05:19:18","post_content":"","post_title":"JOURNAL OF CHROMATOGRAPHY A","post_excerpt":"","post_status":"publish","comment_status":"closed","ping_status":"closed","post_password":"","post_name":"journal-of-chromatography-a-2","to_ping":"","pinged":"","post_modified":"2018-12-04 06:19:18","post_modified_gmt":"2018-12-04 05:19:18","post_content_filtered":"","post_parent":0,"guid":"https:\/\/aprifel-pp.mentalworks.biz\/fr\/source\/journal-of-chromatography-a-2\/","menu_order":0,"post_type":"source","post_mime_type":"","comment_count":"0","filter":"raw"}]},"yoast_head":"<!-- This site is optimized with the Yoast SEO Premium plugin v23.6 (Yoast SEO v23.6) - 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